| Oxford Diffraction Xcalibur Eos diffractometer | 1306 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 1265 reflections with I > 2σ(I) |
| graphite | Rint = 0.032 |
| Detector resolution: 16.1544 pixels mm-1 | θmax = 75.7°, θmin = 7.4° |
| ω scans | h = −12→13 |
| Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2009) | k = −8→8 |
| Tmin = 0.640, Tmax = 1.000 | l = −11→12 |
| 2817 measured reflections |
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