| Bruker SMART APEXII diffractometer | 1342 independent reflections |
| Radiation source: fine-focus sealed tube | 1096 reflections with I > 2σ(I) |
| graphite | Rint = 0.028 |
| φ and ω scans | θmax = 26.4°, θmin = 2.3° |
| Absorption correction: numerical (SADABS; Sheldrick, 2002) | h = −6→6 |
| Tmin = 0.501, Tmax = 0.851 | k = −9→8 |
| 4678 measured reflections | l = −19→21 |