Rigaku AFC10/Saturn724+ diffractometer	2973 reflections with I > 2σ(I)
Radiation source: Rotating Anode	Rint = 0.028
graphite	θmax = 27.5°, θmin = 3.3°
Detector resolution: 28.5714 pixels mm-1	h = −9→8
phi and ω scans	k = −12→13
18847 measured reflections	l = −38→38
3143 independent reflections