| Bruker APEXII CCD diffractometer | 4252 independent reflections |
| Radiation source: fine-focus sealed tube | 2225 reflections with I > 2σ(I) |
| graphite | Rint = 0.065 |
| φ and ω scans | θmax = 26.5°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −11→11 |
| Tmin = 0.983, Tmax = 0.987 | k = −13→12 |
| 8475 measured reflections | l = −13→13 |