Oxford Diffraction Xcalibur Ruby Gemini diffractometer | 5437 independent reflections |
Radiation source: Enhance (Cu) X-ray Source | 3425 reflections with I > 2σ(I) |
graphite | Rint = 0.032 |
Detector resolution: 10.5081 pixels mm-1 | θmax = 73.6°, θmin = 5.3° |
ω scans | h = −5→8 |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) | k = −15→14 |
Tmin = 0.896, Tmax = 1.000 | l = −20→20 |
9440 measured reflections |