| Bruker APEX DUO CCD area-detector diffractometer | 7670 independent reflections |
| Radiation source: sealed tube | 6483 reflections with I > 2σ(I) |
| graphite | Rint = 0.036 |
| φ and ω scans | θmax = 32.5°, θmin = 2.7° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −14→14 |
| Tmin = 0.873, Tmax = 0.962 | k = −9→9 |
| 30082 measured reflections | l = −52→52 |