| Bruker APEXII CCD area-detector diffractometer | 2072 independent reflections |
| Radiation source: fine-focus sealed tube | 1184 reflections with I > 2σ(I) |
| graphite | Rint = 0.080 |
| φ and ω scans | θmax = 25.0°, θmin = 2.3° |
| Absorption correction: multi-scan (SADABS; Bruker, 2006) | h = −17→17 |
| Tmin = 0.564, Tmax = 0.564 | k = −17→17 |
| 14047 measured reflections | l = −13→13 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.