Skip to main content
. 2011 Jan 15;67(Pt 2):o403–o404. doi: 10.1107/S1600536811001589
O1A—C2A 1.286 (2) N1B—H1NB 1.00 (2)
N1A—C1A 1.350 (2) N2B—C2B 1.356 (2)
N1A—N2A 1.372 (2) N2B—H2NB 1.02 (3)
N1A—H1NA 0.98 (2) C1B—C3B 1.386 (3)
N2A—C2A 1.353 (2) C1B—C10B 1.497 (3)
N2A—H2NA 0.98 (3) C2B—C3B 1.427 (2)
C1A—C3A 1.382 (2) C3B—C4B 1.471 (3)
C1A—C10A 1.500 (2) C4B—C5B 1.394 (3)
C2A—C3A 1.428 (2) C4B—C9B 1.401 (3)
C3A—C4A 1.478 (2) C5B—C6B 1.391 (3)
C4A—C5A 1.394 (3) C5B—H5BA 0.9300
C4A—C9A 1.396 (3) C6B—C7B 1.391 (3)
C5A—C6A 1.395 (3) C6B—H6BA 0.9300
C5A—H5AA 0.9300 C7B—C8B 1.383 (4)
C6A—C7A 1.371 (4) C7B—H7BA 0.9300
C6A—H6AA 0.9300 C8B—C9B 1.379 (3)
C7A—C8A 1.381 (4) C8B—H8BA 0.9300
C7A—H7AA 0.9300 C9B—H9BA 0.9300
C8A—C9A 1.391 (3) C10B—C11C 1.403 (3)
C8A—H8AA 0.9300 C10B—C11B 1.408 (3)
C9A—H9AA 0.9300 C10B—H10A 0.9700
C10A—C11A 1.520 (3) C10B—H10B 0.9700
C10A—H10C 0.9700 C10B—H10E 0.9700
C10A—H10D 0.9700 C10B—H10F 0.9700
C11A—H11D 0.9600 C11B—H11A 0.9600
C11A—H11E 0.9600 C11B—H11B 0.9600
C11A—H11F 0.9600 C11B—H11C 0.9600
O1B—C2B 1.283 (2) C11C—H11G 0.9600
N1B—C1B 1.352 (2) C11C—H11H 0.9600
N1B—N2B 1.372 (2) C11C—H11I 0.9600
C1A—N1A—N2A 108.56 (15) N1B—N2B—H2NB 123.0 (14)
C1A—N1A—H1NA 131.6 (14) N1B—C1B—C3B 109.01 (16)
N2A—N1A—H1NA 115.8 (14) N1B—C1B—C10B 121.27 (19)
C2A—N2A—N1A 109.22 (15) C3B—C1B—C10B 129.69 (19)
C2A—N2A—H2NA 128.0 (15) O1B—C2B—N2B 122.08 (16)
N1A—N2A—H2NA 121.5 (15) O1B—C2B—C3B 131.19 (16)
N1A—C1A—C3A 108.78 (15) N2B—C2B—C3B 106.72 (16)
N1A—C1A—C10A 120.80 (16) C1B—C3B—C2B 106.31 (16)
C3A—C1A—C10A 130.40 (16) C1B—C3B—C4B 127.96 (17)
O1A—C2A—N2A 122.23 (16) C2B—C3B—C4B 125.72 (17)
O1A—C2A—C3A 130.95 (17) C5B—C4B—C9B 117.91 (18)
N2A—C2A—C3A 106.82 (15) C5B—C4B—C3B 120.77 (16)
C1A—C3A—C2A 106.39 (15) C9B—C4B—C3B 121.31 (18)
C1A—C3A—C4A 128.76 (15) C6B—C5B—C4B 120.9 (2)
C2A—C3A—C4A 124.86 (16) C6B—C5B—H5BA 119.5
C5A—C4A—C9A 118.53 (19) C4B—C5B—H5BA 119.5
C5A—C4A—C3A 120.08 (18) C5B—C6B—C7B 120.0 (2)
C9A—C4A—C3A 121.37 (17) C5B—C6B—H6BA 120.0
C4A—C5A—C6A 120.4 (2) C7B—C6B—H6BA 120.0
C4A—C5A—H5AA 119.8 C8B—C7B—C6B 119.7 (2)
C6A—C5A—H5AA 119.8 C8B—C7B—H7BA 120.1
C7A—C6A—C5A 120.3 (2) C6B—C7B—H7BA 120.1
C7A—C6A—H6AA 119.8 C9B—C8B—C7B 120.1 (2)
C5A—C6A—H6AA 119.8 C9B—C8B—H8BA 119.9
C6A—C7A—C8A 120.2 (2) C7B—C8B—H8BA 119.9
C6A—C7A—H7AA 119.9 C8B—C9B—C4B 121.3 (2)
C8A—C7A—H7AA 119.9 C8B—C9B—H9BA 119.3
C7A—C8A—C9A 120.0 (2) C4B—C9B—H9BA 119.3
C7A—C8A—H8AA 120.0 C11C—C10B—C1B 120.6 (3)
C9A—C8A—H8AA 120.0 C11B—C10B—C1B 117.2 (2)
C8A—C9A—C4A 120.6 (2) C11B—C10B—H10A 108.0
C8A—C9A—H9AA 119.7 C1B—C10B—H10A 108.0
C4A—C9A—H9AA 119.7 C11B—C10B—H10B 108.0
C1A—C10A—C11A 114.22 (16) C1B—C10B—H10B 108.0
C1A—C10A—H10C 108.7 H10A—C10B—H10B 107.2
C11A—C10A—H10C 108.7 C11C—C10B—H10E 107.2
C1A—C10A—H10D 108.7 C1B—C10B—H10E 107.2
C11A—C10A—H10D 108.7 C11C—C10B—H10F 107.2
H10C—C10A—H10D 107.6 C1B—C10B—H10F 107.2
C10A—C11A—H11D 109.5 H10E—C10B—H10F 106.8
C10A—C11A—H11E 109.5 C10B—C11B—H11A 109.5
H11D—C11A—H11E 109.5 C10B—C11B—H11B 109.5
C10A—C11A—H11F 109.5 C10B—C11B—H11C 109.5
H11D—C11A—H11F 109.5 C10B—C11C—H11G 109.5
H11E—C11A—H11F 109.5 C10B—C11C—H11H 109.5
C1B—N1B—N2B 108.18 (15) H11G—C11C—H11H 109.5
C1B—N1B—H1NB 128.5 (13) C10B—C11C—H11I 109.5
N2B—N1B—H1NB 114.6 (14) H11G—C11C—H11I 109.5
C2B—N2B—N1B 109.63 (15) H11H—C11C—H11I 109.5
C2B—N2B—H2NB 126.9 (14)
C1A—N1A—N2A—C2A 5.0 (2) N2B—N1B—C1B—C3B 4.0 (2)
N2A—N1A—C1A—C3A −3.5 (2) N2B—N1B—C1B—C10B −177.96 (18)
N2A—N1A—C1A—C10A 177.71 (17) N1B—N2B—C2B—O1B −179.06 (15)
N1A—N2A—C2A—O1A 175.93 (17) N1B—N2B—C2B—C3B 1.65 (18)
N1A—N2A—C2A—C3A −4.4 (2) N1B—C1B—C3B—C2B −2.9 (2)
N1A—C1A—C3A—C2A 0.8 (2) C10B—C1B—C3B—C2B 179.2 (2)
C10A—C1A—C3A—C2A 179.43 (19) N1B—C1B—C3B—C4B 177.89 (17)
N1A—C1A—C3A—C4A −179.05 (19) C10B—C1B—C3B—C4B 0.1 (3)
C10A—C1A—C3A—C4A −0.4 (3) O1B—C2B—C3B—C1B −178.43 (18)
O1A—C2A—C3A—C1A −178.1 (2) N2B—C2B—C3B—C1B 0.77 (19)
N2A—C2A—C3A—C1A 2.2 (2) O1B—C2B—C3B—C4B 0.8 (3)
O1A—C2A—C3A—C4A 1.7 (3) N2B—C2B—C3B—C4B 179.96 (16)
N2A—C2A—C3A—C4A −177.92 (18) C1B—C3B—C4B—C5B −134.8 (2)
C1A—C3A—C4A—C5A 138.1 (2) C2B—C3B—C4B—C5B 46.2 (3)
C2A—C3A—C4A—C5A −41.7 (3) C1B—C3B—C4B—C9B 46.4 (3)
C1A—C3A—C4A—C9A −43.5 (3) C2B—C3B—C4B—C9B −132.6 (2)
C2A—C3A—C4A—C9A 136.7 (2) C9B—C4B—C5B—C6B −1.6 (3)
C9A—C4A—C5A—C6A 0.2 (3) C3B—C4B—C5B—C6B 179.5 (2)
C3A—C4A—C5A—C6A 178.6 (2) C4B—C5B—C6B—C7B 0.6 (4)
C4A—C5A—C6A—C7A 0.4 (4) C5B—C6B—C7B—C8B 0.4 (4)
C5A—C6A—C7A—C8A −0.6 (4) C6B—C7B—C8B—C9B −0.2 (4)
C6A—C7A—C8A—C9A 0.2 (4) C7B—C8B—C9B—C4B −0.8 (3)
C7A—C8A—C9A—C4A 0.4 (4) C5B—C4B—C9B—C8B 1.8 (3)
C5A—C4A—C9A—C8A −0.6 (3) C3B—C4B—C9B—C8B −179.4 (2)
C3A—C4A—C9A—C8A −179.0 (2) N1B—C1B—C10B—C11C −22.8 (4)
N1A—C1A—C10A—C11A 33.3 (3) C3B—C1B—C10B—C11C 154.8 (3)
C3A—C1A—C10A—C11A −145.2 (2) N1B—C1B—C10B—C11B −96.9 (3)
C1B—N1B—N2B—C2B −3.53 (19) C3B—C1B—C10B—C11B 80.7 (3)