Rigaku Saturn724 diffractometer | 7270 independent reflections |
Radiation source: Sealed Tube | 6754 reflections with I > 2σ(I) |
Graphite Monochromator | Rint = 0.040 |
Detector resolution: 28.5714 pixels mm-1 | θmax = 28.4°, θmin = 2.6° |
dtprofit.ref scans | h = −14→14 |
Absorption correction: multi-scan (CrystalClear; Rigaku, 2007) | k = −16→15 |
Tmin = 0.873, Tmax = 0.873 | l = −16→16 |
29300 measured reflections |