Bruker APEXII CCD diffractometer | 2673 independent reflections |
Radiation source: fine-focus sealed tube | 2411 reflections with I > 2σ(I) |
graphite | Rint = 0.032 |
φ and ω scans | θmax = 28.3°, θmin = 2.4° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −13→13 |
Tmin = 0.917, Tmax = 0.940 | k = −15→15 |
17626 measured reflections | l = −13→13 |