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. 2011 Feb 12;67(Pt 3):o632. doi: 10.1107/S1600536811004685
Bruker Kappa APEXII diffractometer 5276 independent reflections
Radiation source: fine-focus sealed tube 3696 reflections with I > 2σ(I)
graphite Rint = 0.023
ω and φ scans θmax = 32.8°, θmin = 2.5°
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) h = −15→16
Tmin = 0.536, Tmax = 0.648 k = −23→24
21249 measured reflections l = −12→11