Bruker Kappa APEXII diffractometer | 5276 independent reflections |
Radiation source: fine-focus sealed tube | 3696 reflections with I > 2σ(I) |
graphite | Rint = 0.023 |
ω and φ scans | θmax = 32.8°, θmin = 2.5° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −15→16 |
Tmin = 0.536, Tmax = 0.648 | k = −23→24 |
21249 measured reflections | l = −12→11 |