Table II. Refinement statistics.
EpiD | EpiD-H67N-DSYTC | |
---|---|---|
Resolution range (Å) | 20.0–2.5 | 20.0–2.6 |
Reflections in working set | 77 526 | 53 471 |
Reflections in test set | 4087 (5%) | 2881 (5%) |
Rcryst (%) | 22.1 | 20.9 |
Rfree (%) | 25.5 | 22.6 |
Protein atoms (non-H) | 15 994 | 5608 |
Solvent atoms (non-H) | 416 | 136 |
Cofactor atoms (non-H) | 372 | 124 |
Peptide atoms (non-H) | – | 160 |
Average B-factor (Ų) | 37.3 | 49.5 |
R.m.s. ΔB (Ų) | 1.5 | 1.7 |
Deviations from ideality (r.m.s.) | ||
bond lengths (Å) | 0.008 | 0.008 |
bond angles (°) | 1.29 | 1.29 |