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. 2000 Dec 1;19(23):6299–6310. doi: 10.1093/emboj/19.23.6299

Table II. Refinement statistics.

  EpiD EpiD-H67N-DSYTC
Resolution range (Å) 20.0–2.5 20.0–2.6
Reflections in working set 77 526 53 471
Reflections in test set 4087 (5%) 2881 (5%)
Rcryst (%) 22.1 20.9
Rfree (%) 25.5 22.6
Protein atoms (non-H) 15 994 5608
Solvent atoms (non-H) 416 136
Cofactor atoms (non-H) 372 124
Peptide atoms (non-H) 160
Average B-factor (Ų) 37.3 49.5
R.m.s. ΔB (Ų) 1.5 1.7
Deviations from ideality (r.m.s.)    
 bond lengths (Å) 0.008 0.008
 bond angles (°) 1.29 1.29