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. Author manuscript; available in PMC: 2012 Mar 1.
Published in final edited form as: Bioorg Med Chem. 2011 Jan 15;19(5):1816–1822. doi: 10.1016/j.bmc.2011.01.001

Scheme 1. Syntheses of Desmosdumotin C Derivatives.

Scheme 1

Reagents: a) Prenyl Br, KOH, water for R = Prenyl; RI, NaOMe, MeOH, reflux for others; b) TMSCHN2 for R' = Me; R'I, K2CO3, acetone, reflux for others; c) 50% aq. KOH, EtOH, ArCHO, rt; d) Prenly Br, K2CO3, acetone reflux