Table 3.
Detail runs of fractional factorial design and the responses.
Run | A: DGF (L/min) |
B: NP (psi) |
C: VT (°C) |
D:CV (V) |
E:SLF (µL/min) |
F: DGT (°C) |
S/N(avg) |
Peak area(avg) |
---|---|---|---|---|---|---|---|---|
1 | 2 | 5 | 300 | 3500 | 20 | 150 | 99. | 6.2×105 |
2 | 2 | 5 | 200 | 1500 | 5 | 150 | 82 | 1.0×106 |
3 | 2 | 20 | 300 | 1500 | 5 | 150 | 41 | 2.8×105 |
4 | 10 | 20 | 300 | 1500 | 20 | 150 | 56 | 2.8×105 |
5 | 10 | 5 | 200 | 1500 | 20 | 150 | 48 | 4.5×105 |
6 | 2 | 20 | 200 | 3500 | 20 | 150 | 74 | 7.3×105 |
7 | 10 | 20 | 300 | 3500 | 20 | 200 | 34 | 1.9×105 |
8 | 10 | 5 | 300 | 1500 | 5 | 200 | n.a.a) | n.a.a) |
9 | 10 | 20 | 200 | 1500 | 5 | 200 | 18 | 3.1×105 |
10 | 10 | 5 | 200 | 3500 | 20 | 200 | 24 | 2.8×105 |
11 | 10 | 5 | 300 | 3500 | 5 | 150 | n.a.a) | n.a.a) |
12 | 2 | 20 | 300 | 3500 | 5 | 200 | 24 | 2.2×105 |
13 | 2 | 5 | 200 | 3500 | 5 | 200 | 56 | 4.9×105 |
14 | 2 | 5 | 300 | 1500 | 20 | 200 | 60 | 5.2×105 |
15 | 2 | 20 | 200 | 1500 | 20 | 200 | 83 | 9.9×105 |
16 | 10 | 20 | 200 | 3500 | 5 | 150 | 27 | 1.4×105 |
17 | 6 | 12.5 | 250 | 2500 | 12.5 | 175 | 80 | 2.4×105 |
18 | 6 | 12.5 | 250 | 2500 | 12.5 | 175 | 74 | 3.0×105 |
19 | 6 | 12.5 | 250 | 2500 | 12.5 | 175 | 68 | 2.9×105 |
20 | 6 | 12.5 | 250 | 2500 | 12.5 | 175 | 73 | 2.8×105 |
21 | 6 | 12.5 | 250 | 2500 | 12.5 | 175 | 72 | 2.7×105 |
22 | 6 | 12.5 | 250 | 2500 | 12.5 | 175 | 76 | 2.9×105 |
Data not available duo to ionization problem.