Table 1. Summary of data-collection statistics.

Values in parentheses are for the highest resolution shell.

Data-collection parameters
Wavelength (Å)	0.8123
Temperature (K)	100
Oscillation range (°)	0.8
Crystal-to-detector distance (mm)	256
Data-integration statistics
Space group	P212121
Unit-cell parameters (Å)	a = 103.5, b = 104.1, c = 109.6
Resolution limits (Å)	30–2.60
Total No. of reflections	424031
No. of unique reflections	31741
Multiplicity	5.1 (4.9)
Completeness (%)	95.3 (95.0)
Rmerge†	0.042 (0.48)
Mean I/σ(I)	23.0 (3.3)
Molecules per asymmetric unit	4
VM‡ (Å3 Da−1)	2.85
Solvent content (%)	56

^† R _merge = , where 〈I(hkl)〉 is the mean intensity of the observations I_i(hkl) of reflection hkl.

^‡For four molecules in the asymmetric unit.