Table 1. Summary of diffraction data statistics.
Values in parentheses are for the highest resolution shell.
| cGAPDH + NADP+ | cGAPDH C150S | |
|---|---|---|
| Wavelength (Å) | 0.931 | 0.9795 |
| Space group | I4122 | I4122 |
| Unit-cell parameters (Å, °) | a = b = 90.75, c = 225.48 | a = b = 90.46, c = 222.79 |
| Resolution limits (Å) | 45.4–1.9 (2.0–1.9) | 63.96–1.91 (1.91–1.96) |
| No. of observations | 268069 (38889) | 257750 (12978) |
| No. of unique observations | 37590 (5379) | 36172 (2626) |
| Completeness | 100.0 (100.0) | 100 (99.9) |
| 〈I/σ(I)〉 | 12.9 (4.2) | 14.9 (2.4) |
| Rmerge† | 0.13 (0.43) | 0.102 (0.572) |
R
merge =
, where I
i(hkl) is the intensity of an individual measurement of the reflection with Miller indices hkl and 〈I(hkl)〉 is the mean intensity of this reflection.