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. 2011 Mar 25;67(Pt 4):457–460. doi: 10.1107/S1744309111003113

Table 1. Diffraction data statistics for Drep2 CIDE–Drep3 CIDE complex crystals.

Values in parentheses are for the highest resolution shell.

No. of crystals 1
Beamline BL-4A, PAL
Wavelength (Å) 1.0000
Detector ADSC Quantum 315r
Crystal-to-detector distance (mm) 300
Rotation range per image (°) 1
Total rotation range (°) 180
Exposure time per image (s) 10
Resolution range (Å) 50–5.8
Space group P41
Unit-cell parameters (Å) a = 109.0, b = 109.0, c = 46.2
Mosaicity (°) 0.8
Total No. of measured intensities 90452
No. of unique reflections 3649
Multiplicity 2.8 (2.8)
Mean I/σ(I) 13.9 (2.6)
Completeness (%) 99.2 (92.4)
Rmerge (%) 6.5 (34.4)
Overall B factor from Wilson plot (Å2) 72

R merge = Inline graphic Inline graphic, where Ii(hkl) is the ith observation of reflection hkl and 〈I(hkl)〉 is the weighted average intensity for all observations of reflection hkl.