TABLE 1.
Data collection and refinement statistics
| MGS + lactate | MGS Mg2+ + GDP | MGS Mn2+ + GDP | MGS Mg2+ + GDP-mannose | |
|---|---|---|---|---|
| Data collection | ||||
| Space group | P3221 | P3221 | P3221 | P3221 |
| Cell dimensions | ||||
| a, b, c | 149.0, 149.0, 155.0 Å | 149.6, 149.6, 154.1 Å | 149.8, 149.8, 154.7 Å | 149.5, 149.5, 154.3 Å |
| α, β, γ | 90, 90, 120° | 90, 90, 120° | 90, 90, 120° | 90, 90, 120° |
| Resolution | 67 to 2.30 Å (2.42 to 2.30 Å) | 50 to 2.45 Å (2.54 to 2.45 Å) | 50 to 2.80 Å (2.90 to 2.80 Å) | 23.4 to 2.70 Å (2.85 to 2.70 Å) |
| Rmerge | 0.10 (0.37) | 0.072 (0.52) | 0.075 (0.59) | 0.12 (0.55) |
| I/σI | 7.6 (2.4) | 17.5 (2.9) | 22.3 (3.4) | 9.5 (2.8) |
| Completion | 99.7% (96.8%) | 100% (100%) | 99.9% (100%) | 96.8% (98.8%) |
| Redundancy | 2.6 (2.6) | 6.1 (6.3) | 10.9 (10.7) | 5.4 (5.3) |
| Refinement | ||||
| Rwork/Rfree | 0.20/0.22 | 0.20/0.23 | 0.19/0.22 | 0.19/0.22 |
| Root mean square deviations | ||||
| Bond lengths | 0.017 Å | 0.015 Å | 0.016 Å | 0.016 Å |
| Bond angles | 1.58° | 1.52° | 1.67° | 1.62° |
| PDB codes | 2y4j | 2y4k | 2y4l | 2y4m |