TABLE 1.
Statistics of crystallographic analysis
| Data collection | |
| Space group | P21 |
| Unit cell (Å) | a = 50.640 b = 155.568 c = 97.374 β = 94.70 |
| Resolution (Å) | 50-1.95 |
| Completeness | 96.1 (92.4)a |
| Redundancy | 6.5 (5.2) |
| I/σ(I) | 20.4 (3.6) |
| Rsymb(%) | 10.3 (44.8) |
| Refinement | |
| Resolution | 50-1.95 |
| Rwork/Rfreec(%) | 17.03/20.57 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (°) | 1.106 |
| Ramachandran plot (%)d | |
| Most favored (%) | 91.7 |
| Additionally allowed (%) | 7.8 |
| Generously allowed | 0.5 |
| Disallowed (%) | 0.0 |
a Values in parentheses are for reflections in the highest resolution shell.
b Rsym = ΣhklΣi|I(hkl)i − <I(hkl)>/ΣhklΣI<I(hkl)i> over i observations.
c Value of Rfree for 1.91% of randomly selected reflections excluded from refinement.
d As defined in PROCHECK.