Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.025	Hydrogen site location: difference Fourier map
wR(F2) = 0.065	H-atom parameters constrained
S = 1.15	w = 1/[σ2(Fo2) + (0.0297P)2 + 0.3709P] where P = (Fo2 + 2Fc2)/3
3477 reflections	(Δ/σ)max = 0.001
192 parameters	Δρmax = 0.29 e Å−3
0 restraints	Δρmin = −1.25 e Å−3