| Bruker SMART CCD area-detector diffractometer | 1057 independent reflections |
| Radiation source: fine-focus sealed tube | 867 reflections with I > 2σ(I) |
| graphite | Rint = 0.048 |
| φ and ω scans | θmax = 25.0°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −13→11 |
| Tmin = 0.827, Tmax = 0.894 | k = −6→6 |
| 2778 measured reflections | l = −8→11 |