| Rigaku R-AXIS RAPID CCD diffractometer | 5833 independent reflections |
| Radiation source: rolling anode | 4835 reflections with I > 2σ(I) |
| graphite | Rint = 0.073 |
| Detector resolution: 10.00 pixels mm-1 | θmax = 25.2°, θmin = 3.0° |
| ω scans | h = −14→15 |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | k = −13→12 |
| Tmin = 0.489, Tmax = 0.573 | l = −26→26 |
| 23458 measured reflections |
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