| Oxford Diffraction Xcalibur Eos Gemini diffractometer | 3466 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2802 reflections with I > 2σ(I) |
| graphite | Rint = 0.016 |
| Detector resolution: 16.1500 pixels mm-1 | θmax = 29.1°, θmin = 3.1° |
| φ and ω scans | h = −9→8 |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) | k = −11→11 |
| Tmin = 0.967, Tmax = 1.000 | l = −16→15 |
| 6346 measured reflections |