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. 2011 Apr 16;67(Pt 5):o1158. doi: 10.1107/S1600536811012815
Rigaku Saturn CCD area-detector diffractometer 3527 independent reflections
Radiation source: rotating anode 3320 reflections with I > 2σ(I)
multilayer Rint = 0.053
Detector resolution: 14.63 pixels mm-1 θmax = 27.9°, θmin = 1.5°
ω and φ scans h = −14→15
Absorption correction: multi-scan (CrystalClear; Rigaku, 2005) k = −12→9
Tmin = 0.974, Tmax = 0.991 l = −36→36
25486 measured reflections