Rigaku Saturn CCD area-detector diffractometer | 3527 independent reflections |
Radiation source: rotating anode | 3320 reflections with I > 2σ(I) |
multilayer | Rint = 0.053 |
Detector resolution: 14.63 pixels mm-1 | θmax = 27.9°, θmin = 1.5° |
ω and φ scans | h = −14→15 |
Absorption correction: multi-scan (CrystalClear; Rigaku, 2005) | k = −12→9 |
Tmin = 0.974, Tmax = 0.991 | l = −36→36 |
25486 measured reflections |