| Bruker APEXII DUO CCD area-detector diffractometer | 6956 independent reflections |
| Radiation source: fine-focus sealed tube | 6490 reflections with I > 2σ(I) |
| graphite | Rint = 0.033 |
| φ and ω scans | θmax = 34.0°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −17→17 |
| Tmin = 0.953, Tmax = 0.987 | k = −16→17 |
| 26247 measured reflections | l = −21→21 |