| Siemens SMART CCD area-detector diffractometer | 4356 independent reflections |
| Radiation source: fine-focus sealed tube | 3598 reflections with I > 2σ(I) |
| graphite | Rint = 0.017 |
| phi and ω scans | θmax = 25.0°, θmin = 2.3° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −10→10 |
| Tmin = 0.647, Tmax = 0.793 | k = −13→12 |
| 6566 measured reflections | l = −15→15 |
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