| Rigaku R-AXIS RAPID diffractometer | 2540 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.083 |
| graphite | θmax = 27.0°, θmin = 3.1° |
| Detector resolution: 10.00 pixels mm-1 | h = −19→19 |
| ω scans | k = −14→14 |
| 19199 measured reflections | l = −16→16 |
| 4507 independent reflections |
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