| Rigaku Saturn CCD area-detector diffractometer | 3448 independent reflections |
| Radiation source: rotating anode | 2142 reflections with I > 2σ(I) |
| multilayer | Rint = 0.063 |
| Detector resolution: 14.63 pixels mm-1 | θmax = 27.9°, θmin = 1.3° |
| ω and φ scans | h = −43→41 |
| Absorption correction: multi-scan CrystalClear | k = −14→14 |
| Tmin = 0.982, Tmax = 0.989 | l = −10→10 |
| 18031 measured reflections |