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. 2011 Apr 7;67(Pt 5):o1042. doi: 10.1107/S1600536811011597
Rigaku Saturn CCD area-detector diffractometer 3448 independent reflections
Radiation source: rotating anode 2142 reflections with I > 2σ(I)
multilayer Rint = 0.063
Detector resolution: 14.63 pixels mm-1 θmax = 27.9°, θmin = 1.3°
ω and φ scans h = −43→41
Absorption correction: multi-scan CrystalClear k = −14→14
Tmin = 0.982, Tmax = 0.989 l = −10→10
18031 measured reflections