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. Author manuscript; available in PMC: 2012 Jun 1.
Published in final edited form as: J Pharm Biomed Anal. 2011 Mar 5;55(3):487–493. doi: 10.1016/j.jpba.2011.01.040

Table 4.

Intra- and inter day precision and relative errors (accuracy) for alfentanil and midazolam.

Alfentanil Midazolam
Concentration (ng/ml)
1 10 100 1.35 12 100
Intraday run 1-mean 0.98 9.67 102.7 1.36 10.6 103
SD 0.04 0.77 5.6 0.11 0.5 7
%CV 4.1 8.0 5.4 8.1 5.1 7.2
% RE -2.0 -3.3 2.7 0.7 -11.3 2.9

Intraday run 2-mean 0.99 9.88 97.1 1.39 12.0 102
SD 0.05 0.42 3.2 0.09 0.6 6
%CV 5.1 4.3 3.3 6.5 5.3 5.4
% RE -1.0 -1.2 -2.9 3.0 -0.2 2.3

Intraday run 3-mean 0.98 9.83 97.0 1.32 12.2 105
SD 0.05 0.61 2.8 0.05 0.7 4
%CV 5.1 6.2 2.9 3.8 6.0 3.7
% RE -2.0 -1.7 -3.0 -2.2 1.8 4.6

Interday run-mean 0.98 9.79 98.9 1.36 11.6 103
SD 0.04 0.59 4.7 0.09 0.9 5
%CV 4.1 6.0 4.7 6.6 8.0 5.3
% RE -2.0 -2.1 -1.1 0.7 -3.3 3.3
N 18 18 18 18 18 18