Table I.
Data Collection | |
Space group | P212121 |
Cell dimensions | |
a, b, c (Å) | 60.28, 111.16, 138.93 |
α, β, γ (°) | 90, 90, 90 |
Resolution (Å) | 60.3-2.5 |
Rmerge (%) | 8.0 (38.7) |
I/σI | 16.6 (3.9) |
Completeness (%) | 99.9 (100.0) |
Redundancy | 7.1 |
Refinement | |
Resolution (Å) | 2.5 |
No. Reflections | 31,473 |
Rwork/Rfree (%) | 21.3/26.2 |
No. Atoms | |
Total | 5727 |
Protein | 5547 |
Water | 180 |
Average B-factor (Å2) | |
Total | 16.2 |
Protein | 16.2 |
Water | 16.8 |
R.m.s. Deviations | |
Bond lengths (Å) | 0.003 |
Bond angles (°) | 0.532 |
Ramachandran Analysis | |
Most favored (%) | 89.7 |
Additionally allowed | 10.0 |
Generously allowed | 0.3 |
Values in parenthesis correspond to the highest resolution shell (2.64-2.50 Å)