Table 4.
Intra-day assay precision and accuracy of the HPLC method for the determination of NAG*
Nominal concentration (µg/ml) | Calculated concentration (µg/ml) | Precision RSD (%) | Accuracy error |
---|---|---|---|
1 | 1.02 | 11.27 | 2.17 |
2 | 2.01 | 9.55 | 0.67 |
4 | 4.005 | 7.35 | 0.07 |
6 | 5.96 | 5.76 | 0.70 |
8 | 7.92 | 5.82 | 0.96 |
10 | 10.08 | 6.88 | 0.80 |
Samples were analyzed in five replicates for each concentration per day.