TABLE 2.
Refinement statistics
| Parameters | TBC1D1 | TBC1D4 |
|---|---|---|
| Space group unit cell dimensions | P43212 (a = b = 117.36 Å, c = 141.27 Å) | P3221 (a = b = 151.21 Å, c = 53.16 Å) |
| Resolution range (Å) | 50–2.2 | 50–3.5 |
| Unique reflections (test set) | 50,676 (4,876) | 8,683 (920) |
| Wilson B (Å2) | 38.61 | 143.87 |
| R-factora (Rfree) | 0.199 (0.239) | 0.246 (0.300) |
| No. of scatters (no. of residues) | A 750–821/829–1,066 (310) B 752–1,067 (316) | 875–1,169 (295) |
| No. of water molecules | 409 | 9 |
| r.m.s.d. bonds (Å) | 0.0106 | 0.0133 |
| r.m.s.d. angles (°) | 1.606 | 1.572 |
| Average B-factor (main chain) (Å2) | 44.49 | 101.31 |
| Average B-factor (side chain) (Å2) | 44.95 | 105.58 |
| Average B-factor (water) (Å2) | 51.00 | 62.17 |
a R-factor = Σ(|Fobs| − |Fcalc|)/Σ|Fobs|.