Bruker APEX CCD area-detector diffractometer | 1254 independent reflections |
Radiation source: fine-focus sealed tube | 1172 reflections with I > 2s(I) |
graphite | Rint = 0.022 |
Frames, each covering 0.3 ° in ω scans | θmax = 25.5°, θmin = 1.7° |
Absorption correction: multi-scan (SADABS; Bruker, 2003) | h = −30→30 |
Tmin = 0.916, Tmax = 1.000 | k = −5→5 |
7171 measured reflections | l = −13→13 |