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. 2011 Mar 5;67(Pt 4):o787. doi: 10.1107/S1600536811007471
Bruker APEX CCD area-detector diffractometer 1254 independent reflections
Radiation source: fine-focus sealed tube 1172 reflections with I > 2s(I)
graphite Rint = 0.022
Frames, each covering 0.3 ° in ω scans θmax = 25.5°, θmin = 1.7°
Absorption correction: multi-scan (SADABS; Bruker, 2003) h = −30→30
Tmin = 0.916, Tmax = 1.000 k = −5→5
7171 measured reflections l = −13→13