Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| O1—H1⋯N4 | 0.82 | 1.93 | 2.643 (8) | 145 |
| N1—H1A⋯Br2 | 0.91 (8) | 2.69 (7) | 3.081 (7) | 107 (6) |
| O2—H2⋯O9i | 0.82 | 1.85 | 2.660 (15) | 167 |
| O3—H3⋯N2 | 0.82 | 1.93 | 2.661 (9) | 148 |
| N3—H3B⋯Br4 | 0.91 (8) | 2.77 (8) | 3.097 (7) | 103 (5) |
| O4—H4⋯O6ii | 0.82 | 2.13 | 2.721 (10) | 129 |
| O5—H5⋯N6 | 0.82 | 1.95 | 2.650 (9) | 143 |
| N5—H5B⋯Br5 | 0.90 (6) | 2.77 (8) | 3.110 (7) | 104 (6) |
| O6—H6⋯O8iii | 0.82 | 1.95 | 2.735 (9) | 160 |
| O7—H7⋯N8 | 0.85 (6) | 1.99 (8) | 2.717 (9) | 142 (6) |
| N7—H7B⋯Br7 | 0.90 (6) | 2.61 (8) | 3.100 (7) | 115 (6) |
| O8—H8⋯O2iv | 0.84 (9) | 1.90 (8) | 2.713 (11) | 162 (8) |
| O9—H9⋯O10v | 0.82 | 2.18 | 2.94 (2) | 156 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
.