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. Author manuscript; available in PMC: 2012 Mar 30.
Published in final edited form as: J Am Chem Soc. 2011 Mar 4;133(12):4359–4366. doi: 10.1021/ja107775w

Figure 2.

Figure 2

13C-13C DQ spectra of U-DsbB(C41S) at 10.0 kHz MAS with (a) 0.8 ms and (b) 1.2 ms POST-C7 mixing (B0 = 14.1 T, Tsample = −12 °C, 2 s pulse delay, maximum t1 = 10.24 ms, maximum t2 = 20.48 ms). Blue contours represent one-bond correlations and red contours represent two-bond correlations with the opposite sign. (c) UQ-8 structure with highlights of one-bond (blue lines) and two-bond (red arrows) correlations observed in DQ experiments.