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. Author manuscript; available in PMC: 2012 Mar 30.
Published in final edited form as: J Am Chem Soc. 2011 Mar 4;133(12):4359–4366. doi: 10.1021/ja107775w

Figure 4.

Figure 4

Expansions of the 13C-13C 2D correlation spectra of FLYPW-DsbB(C41S) samples at pH (a) 5.5 and (b) 8.0 with 100 ms DARR mixing and 1.8 ms 15N REDOR dephasing under 13.333 kHz MAS (B0 = 14.1 T, Tsample = −16.6 °C, 1.5 s pulse delay, maximum t1 = 10.24 ms, maximum t2 = 20.48 ms). Crosspeaks between methoxys (C2′ and C3′) and carbonyls (C1 and C4) or double-bonded carbons (C2 and C3) are marked.