Table 1.

¹H and ¹³C NMR Data of Compounds 1 and 2

#	1 (1H)a	2 (1H)a	2 (1H)b	#	1 (13C)c	2 (13C)d
1				1	155.7	154.7
2				2	141.4	142.7
3				3	157.9	154.4
4	7.27 (s)	7.27 (s)	7.25/7.27 (s)	4	104.3	107.3/107.7
5				5	127.6	129.5/130.5
6				6	182.5	182.8
7				7	141.3	140.8
8				8	140.4	140.8
9				9	187.5	189.9
10				10	110.7	111.9
1′	2.79 (d 20.1)	2.78 (d 19.8)	2.63/2.67 (d 19.8)	1′	31.7	32.3
	2.53 (d 20.1)	2.52 (d 19.8)	2.41/2.43 (d 19.8)
2′				2′	96.0	96.8
3′	1.80 (m)	1.77 (m)	1.73 (m)	3′	42.2	42.8
4′	1.2~1.6 (m)	1.2~1.6 (m)	1.2~1.6 (m)	4′	22.6	23.7
5′	1.2~1.6 (m)	1.2~1.6 (m)	1.2~1.6 (m)	5′	30.6	31.0
6′	1.2~1.6 (m)	1.2~1.6 (m)	1.2~1.6 (m)	6′	29.7	30.8
7′	1.2~1.6 (m)	1.2~1.6 (m)	1.2~1.6 (m)	7′	29.2	30.4
8′	1.2~1.6 (m)	1.2~1.6 (m)	1.2~1.6 (m)	8′	23.0	24.5
9′	0.90 (t 6.6)	0.88 (t 6.6)	0.91 (t 6.6)	9′	14.1	14.4
1″	4.73 (d 18.6)	4.71 (d 18.6)	4.59 (m)	1″	56.5	56.5
	4.68 (d 18.6)	4.66 (d 18.6)
1-OH	12.05	11.90 (s)
2-OCH3	4.05 (s)			2-OCH3	61.0
3-OCH3	3.99 (s)	4.01 (s)	3.94/3.90 (s)	3-OCH3	57.4	58.1

^aδ (ppm) 500 MHz in CDCl₃; multiplicities; J values (Hz) in parentheses.

^bδ (ppm) 500 MHz in CD₃OD; multiplicities; J values (Hz) in parentheses.

^cδ (ppm) 150 MHz in CDCl₃.

^dδ (ppm) 150 MHz in CD₃OD.