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. Author manuscript; available in PMC: 2012 May 25.
Published in final edited form as: J Am Chem Soc. 2011 May 3;133(20):7700–7703. doi: 10.1021/ja2023898

Table 2.

Synthesis of tripeptides.a

graphic file with name nihms294143u3.jpg
Entry Dipeptide Isonitrile Product Yield
1 13 graphic file with name nihms294143t10.jpg
16 		graphic file with name nihms294143t11.jpg
19 		65%
2 14 graphic file with name nihms294143t12.jpg
16 		graphic file with name nihms294143t13.jpg
20 		55%
3 15 graphic file with name nihms294143t14.jpg
16 		graphic file with name nihms294143t15.jpg
21 		55%
4 12 graphic file with name nihms294143t16.jpg
22 		graphic file with name nihms294143t17.jpg
23 		52%
5 15 graphic file with name nihms294143t18.jpg
22 		graphic file with name nihms294143t19.jpg
24 		53%
a

Key: (a) microwave, 120 °C, CHCl3, 2,6-dimethyl thiophenol.