Table 1.
Data collection and refinement statistics
| Measurement | Value |
|---|---|
| Space group | P212121 |
| Unit cell | a = 59.51 Å; b = 59.84 Å; c = 68.98 Å |
| Resolution, Å | 21–2.3 |
| Unique reflections | 9874 |
| Overall completeness, % | 87.1 |
| Last resolution shell completeness, % | 86.3 |
| Rsym, % | 12.7 |
| Multiplicity | 3.7 |
| 〈I/σ〉 | 3.6 |
| Reflections in working set | 8679 |
| Reflections in test set | 890 (8%) |
| Rcryst/Rfree, % | 22.9/28.9 |
| Protein atoms | 2222 |
| Water molecules | 144 |
| rms deviations on bond lengths, Å | 0.01 |
| rms deviations on bond angles, ° | 1.81 |