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. Author manuscript; available in PMC: 2012 Apr 29.
Published in final edited form as: J Org Chem. 2010 Oct 29;75(22):7863–7868. doi: 10.1021/jo101793r

Table 1.

Investigation of Scope in Heterocycle

graphic file with name nihms276459u2.jpg
entry azine ArBr product yield (%)a
1 graphic file with name nihms276459t1.jpg graphic file with name nihms276459t2.jpg 1a 53
2 graphic file with name nihms276459t3.jpg 1b 51
3 graphic file with name nihms276459t4.jpg 1c 78
4 graphic file with name nihms276459t5.jpg 1d 70
5 graphic file with name nihms276459t6.jpg 1e 76
6 graphic file with name nihms276459t7.jpg 1f 67
7 graphic file with name nihms276459t8.jpg 1g 0
8 graphic file with name nihms276459t9.jpg 1h 86b
9 graphic file with name nihms276459t10.jpg 1i 65b
10 graphic file with name nihms276459t11.jpg graphic file with name nihms276459t12.jpg 1j 73b
11 graphic file with name nihms276459t13.jpg 1k 49c
12 graphic file with name nihms276459t14.jpg 1l 24b
13 graphic file with name nihms276459t15.jpg 1m 26b
14 graphic file with name nihms276459t16.jpg 1n 33b
a

Isolated yield of analytically pure product; 0.4 mmol scale in ArBr; 0.8 M absolute concentration in ArBr;

b

Reaction run at 175 °C and 0.3 M absolute concentration in ArBr;

c

Reaction run at 165 °C and 0.3 M absolute concentration in ArBr.