Bruker SMART APEXII DUO CCD area-detector diffractometer | 1784 independent reflections |
Radiation source: fine-focus sealed tube | 1506 reflections with I > 2σ(I) |
graphite | Rint = 0.032 |
φ and ω scans | θmax = 26.5°, θmin = 2.1° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −8→8 |
Tmin = 0.942, Tmax = 0.984 | k = −8→8 |
6312 measured reflections | l = −12→12 |