| Bruker APEXII diffractometer | 1781 reflections with I > 2σ(I) |
| graphite | Rint = 0.025 |
| CCD rotation images, thin slices scans | θmax = 27.5°, θmin = 3.2° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2002) | h = −11→7 |
| Tmin = 0.898, Tmax = 0.987 | k = −6→6 |
| 7993 measured reflections | l = −28→28 |
| 2004 independent reflections |