Table 1.
Compound | Melting point[b] (°C) | Yield[c]% |
---|---|---|
4a | 197–198(197–198) [12,28] | 75 |
4b | 168–171 | 75 |
4c | 206–208(207–209) [12,28] | 75 |
4d | 184–186(184–186) [29] | 70 |
4e | 200–202(201–201) [29] | 75 |
4f | 130–133 | 60 |
4g | oil | 70 |
4h | oil | 60 |
4i | 180–183 | 55 |
4j | 185–188 | 50 |
4k | oil | 65 |
4l | oil | 59 |
3 hours
Experimental
Isolated pure product.