Figure 4. 13C 1D spectra of MSP1D1 in POPC Nanodiscs.
Spectra were acquired on U-13C,15N-labeled MSP1D1 at 8 °C. 13C 1D spectra were acquired with a 1 ms T2 filer, a 0.4 ms HC contact time, where 1H-1H mixing time was incremented and sequentially set to 3 μs, 1 ms, 3 ms, 10 ms and 30 ms. The data were processed with 30 Hz Lorentzian-to-Gaussian line broadening.