Table 1. Crystallization, data collection, and refinement statistics for the SMYD3/Sinefungin structure.
| Space group | P21 |
| Unit Cell | a = 58.175Å,b = 118.073Å,c = 82.901Å,α = γ = 90°,β = 91.579° |
| Wavelength (Å) | 1.2815 |
| Resolution (Å) | 30.0–1.85 |
| Redundancy | 7.3 |
| Unique Reflections | 94,957 |
| Completeness (%) | 99.8 (99.9)a |
| <I/σ (I)> | 18.4 (4.1) |
| Molecules/Assym. Unit | 2 |
| R/Rwork/ Rfree b (%) | 20.1/20.0/21.6 |
a
Numbers in parentheses refer to the highest resolution shell.
b
R = Σ|Fo-Fc|/Σ|Fo|, where Fo and Fc are the observed and calculated structure factors, respectively. Rwork is calculated using the formula for R, but employing only the 95% of reflections used in the refinement and Rfree is calculated using a randomly-selected 5% subset of reflections not used in the refinement.