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Synthetic scheme for the synthesis of radiolabeled 18F-TCO, 618F; Reagents and conditions: a) NaH, ICH2CO2H, reflux, 4h, (THF); b) LiAlH4, 0 °C to rt, 24h, (Et2O); c) hν, rt, 8h, (Et2O/hexanes); d) TsCl, Et3N, rt, 2 h, (MeCN); e) TBAF, rt, 2 h, (THF).
