Table 2.
Entry | R1 | R2 | R3 | Time (h) | Product | Yielda (%) |
---|---|---|---|---|---|---|
1 | H | H | H | 3.0 | 3a | 75 |
2 | CH3 | H | H | 2.5 | 3b | 73 |
3 | CH3 | CH3 | H | 2.5 | 3c | 76 |
4 | OCH3 | H | H | 2.0 | 3d | 75 |
5 | CN | H | H | 4.0 | 3e | 71 |
6 | OH | Br | Br | 3.0 | 3f | 78 |
7 | OH | Cl | Cl | 3.0 | 3g | 76 |
H | 4.0 | 3h | 75 |
Isolated yield.