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. Author manuscript; available in PMC: 2012 Aug 24.
Published in final edited form as: Tetrahedron Lett. 2011 Aug 24;52(34):4375–4377. doi: 10.1016/j.tetlet.2011.05.114

Table 2.

Reaction of various aromatic amines with di-(carboxymethyl)-trithiocarbonyl

graphic file with name nihms-305953-t0003.jpg


Entry R1 R2 R3 Time (h) Product Yielda (%)
1 H H H 3.0 3a 75
2 CH3 H H 2.5 3b 73
3 CH3 CH3 H 2.5 3c 76
4 OCH3 H H 2.0 3d 75
5 CN H H 4.0 3e 71
6 OH Br Br 3.0 3f 78
7 OH Cl Cl 3.0 3g 76
graphic file with name nihms-305953-t0004.jpg H 4.0 3h 75
a

Isolated yield.