Table 1.
Crystallographic parameters for TbGNA1a
| Parameter | Value(s) for TbGNA1b |
|---|---|
| Data collection statistics | |
| Space group | P212121 |
| Unit cell dimensions | |
| a (Å) | 50.86 |
| b (Å) | 64.44 |
| c (Å) | 82.77 |
| Alpha (°) | 90.00 |
| Beta (°) | 90.00 |
| Gamma (°) | 90.00 |
| Wavelength | 1.5418 |
| Resolution range (Å) | 40–1.86 |
| No. of unique reflections | 23,634 |
| No. of reflections observed | 23,625 |
| Rsym | 0.049 (0.237) |
| I/σ〈I〉 | 28.94 (7.5) |
| Completeness (%) | 99.9 (99.9) |
| Redundancy | 7.0 (6.9) |
| Refinement statistics | |
| Resolution range | 35.96–1.86 (1.91–1.86) |
| No. of reflections | 22,408 (1,628) |
| No. of reflections in test set | 1,217 (95) |
| Rwork/Rfree | 0.243/0.282 (0.309/0.331) |
| No. of atoms | |
| Protein | 2,265 |
| Water | 238 |
| Mean B factor (Å2) | 20.24 |
| Ramachandran (%) | |
| Favored | 98.15 |
| Allowed | 1.85 |
| Disallowed | 0 |
| RMSD | |
| Bond length (Å) | 0.002 |
| Bond angle (°) | 0.531 |
a
PDB accession number 3I3G.
b
Values in parentheses are for outer shell.