Table 1. Data-collection statistics.
Crystallization conditions | 0.2 M ammonium sulfate, 23% PEG 4000, 0.1 M MES pH 6.5 |
Wavelength (Å) | 1.5418 |
Temperature (K) | 100 |
Resolution range (Å) | 24.41–2.80 (2.95–2.80) |
Space group | P1 |
Unit-cell parameters (Å, °) | a = 104.29, b = 118.12, c = 121.11, α = 62.66, β = 69.48, γ = 70.74 |
Observed reflections | 307989 (26823) |
Unique reflections | 114916 (16491) |
Data completeness (%) | 99.1 (96.9) |
Multiplicity | 2.7 (1.6) |
〈I/σ(I)〉 | 9.2 (3.7) |
Rmerge (%) | 0.085 (0.167) |
Matthews coefficient (Å3 Da−1) | 2.58 |
Solvent content (%) | 52.32 |