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. 2011 Jul 20;67(Pt 8):911–913. doi: 10.1107/S1744309111022627

Table 1. Data-collection statistics.

Values in parentheses are for the highest resolution shell.

Crystallization conditions 0.2 M ammonium sulfate, 23% PEG 4000, 0.1 M MES pH 6.5
Wavelength (Å) 1.5418
Temperature (K) 100
Resolution range (Å) 24.41–2.80 (2.95–2.80)
Space group P1
Unit-cell parameters (Å, °) a = 104.29, b = 118.12, c = 121.11, α = 62.66, β = 69.48, γ = 70.74
Observed reflections 307989 (26823)
Unique reflections 114916 (16491)
Data completeness (%) 99.1 (96.9)
Multiplicity 2.7 (1.6)
I/σ(I)〉 9.2 (3.7)
Rmerge (%) 0.085 (0.167)
Matthews coefficient (Å3 Da−1) 2.58
Solvent content (%) 52.32