| Oxford Diffraction Xcalibur Sapphire3 Gemini ultra CCD diffractometer | 4791 independent reflections |
| Radiation source: Enhance Ultra (Cu) X-ray Source | 3521 reflections with I > 2σ(I) |
| mirror | Rint = 0.031 |
| Detector resolution: 16.0288 pixels mm-1 | θmax = 62.8°, θmin = 3.6° |
| ω scans | h = −12→12 |
| Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2010) | k = −12→13 |
| Tmin = 0.392, Tmax = 1.000 | l = −14→14 |
| 8708 measured reflections |
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